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LOR 30B process recipe

LOR 30B is the thickest grade in the B series at 1.60-4.35 µm, for lift-off of depositions heavy enough that a two-micron sacrificial film would not break cleanly.

https://nanyte.com/photoresists/lor-30b · last updated 2026-09-12

At a glance
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Manufacturer
MicroChem (MCC) — now Kayaku Advanced Materials
Tone
Not photoimageable (underlayer)
Chemistry
Ancillary (not photoimageable)
Thickness
1.6–4.3 µm
Exposure dose
Not exposed — dissolves in developer
Developer
No specific commercial developer product is named for this grade; the datasheet states LOR/PMGI is compatible with both metal-ion-free (TMAH) and metal-ion-bearing developer chemistries.
Applications
Lift-off

Cross-checked — two independent extractions agree on the spin curve and the single-value figures.

The underlayer is never exposed: it sits beneath an imaged top resist and the developer undercuts it laterally, leaving the overhang lift-off relies on. Schematic cross-sections for LOR 30B — feature width, film aspect ratio and sidewall angle are illustrative, not to scale.
01 / Coating

Spin coating

Spin curve for LOR 30B: film thickness in µm against spin speed in rpm.123451k2k3k4kSPIN SPEED (rpm)THICKNESS (µm)
Data points
LOR 30B — film thickness (µm) by spin speed (rpm)
Seriesrpmµm
LOR 30B10004.3
15003.2
20002.6
25002.1
30001.9
35001.7
40001.6

Values are the manufacturer’s starting points, not a guarantee — characterize on your own tool. Series digitized from a published figure are approximate (±10 %).

read from figure — the purple cross-marker trace legended LOR 30B on the 'Thickness vs. Spin Speed - LOR B Thick Series' chart, p.5, the highest of the five traces. Seven plotted markers at 500 rpm intervals; no numeric table accompanies the chart.

Redrawn from the manufacturer's published data — hover to read between points, click to pin.
  • The topmost trace on the B-series chart and the steepest at the slow end: 43,500 Å at 1000 rpm drops to 25,800 Å by 2000 rpm, then flattens toward 16,000 Å at 4000 rpm.
  • Reaching the top of the range means spinning slowly, where thickness is most sensitive to speed and to dispense, so a target above about 4 µm is worth confirming on a test wafer rather than reading off the chart.
  • Coating parameters are published for the product line rather than per grade: 5 ml dispensed dynamically over 3-5 s onto a 150 mm wafer at 300-500 rpm, 10,000 rpm/s acceleration to a 3,000 rpm terminal speed, 45 s spin, with EBR PG for edge-bead and whisker removal.
Adhesion
HMDS not required — "Primers, such as HMDS, are typically not required" when LOR/PMGI is used as recommended; the datasheet describes excellent adhesion across semiconductor substrates. To dehydrate the surface first, bake at 200 °C for 5 min. LOR/PMGI is virtually insoluble in typical photoresist solvents, so a properly baked underlayer does not intermix with the imaging resist above it.
02 / Bake

Soft bake

Soft bake
Not published — characterize on-tool
Notes
The prebake dries the film and fixes its dissolution and undercut rate, and no grade-specific temperature or time is published. The recommended prebake range for the product line is 160-210 °C, hotplate preferred, and some PMGI products bake as high as 280 °C. Prebake temperature has the greatest influence on undercut rate, with prebake time, developer choice, develop mode and especially develop time behind it. This is the thickest film in the B line, so bake time carries more weight here than on any other B grade — there is several times more solvent to drive out than in a sub-micron coat, and the published undercut-versus-bake curves (Figures 5a and 5b) were measured on LOR 10B, a film roughly a third this thickness.
SOURCE: "Soft-Bake/Prebake Process" section and Figures 5a-5b, Kayaku…

"Soft-Bake/Prebake Process" section and Figures 5a-5b, Kayaku "LOR and PMGI Resists" technical data sheet, Rev. D (August 2023)

03 / Exposure

Exposure

LOR 30B is not photoimageable. It is not exposed at all — it is coated beneath an imaged top resist and undercut laterally during development. See the development step below.

04 / Development

Development

Developer
No specific commercial developer product is named for this grade; the datasheet states LOR/PMGI is compatible with both metal-ion-free (TMAH) and metal-ion-bearing developer chemistries.
Developer family
TMAH or buffered alkaline

Not published for this resist: Dilution, Time, Method, Rinse — characterize on-tool.

SOURCE: Product description, the LOR/PMGI process-flow section and the…

Product description, the LOR/PMGI process-flow section and the product selection guide, Kayaku "LOR and PMGI Resists" technical data sheet, Rev. D (August 2023)

05 / Post-processing

Hard bake, etch & strip

Stripper
Remover PG — expect the long end of any strip time at this thickness. EBR PG removes edge beads and whiskers and is also an effective spin-bowl cleaner and a rework solvent for unbaked wafers.
Storage
Store upright in original sealed containers in a dry area between 4 and 27 °C (40-80 °F), away from ignition sources, light, heat, oxidants, acids and reducers. Do not use after the expiration date.

Not published for this resist: Hard bake, Descum, Etch resistance — characterize on-tool.

06 / Applications

Where it's used

Practical notes from the datasheet

LOR 30B is the thickest sacrificial underlayer in the B series, a PMGI-based film spun beneath a conventional photoresist and never exposed. The reasoning for reaching this far up the range is geometric: a lift-off works when the metal on the substrate and the metal on top of the imaging resist never join, so the underlayer has to be comfortably thicker than the film being deposited, and below that it tears rather than releases. Going thicker than needed is not free — a fast-dissolving B-series film keeps undercutting for as long as the develop runs, and on a 4 µm coat that ledge can travel a long way, which is why the thick-film examples in this datasheet are drawn with features measured in tens of microns rather than fractions of one. Worth knowing before specifying it: the current revision also offers a C series reaching comparable thicknesses at a different dissolution rate, so thickness alone no longer picks the grade.

07 / Family

Grades in this family

Other grades in the LOR B series line differ mainly in coating thickness:

LOR B series — grade comparison
GradeThickness
LOR 7B0.3–0.9 µm
LOR 10B0.7–1.6 µm
LOR 15B1–2.2 µm
LOR 20B1.3–3.5 µm
LOR 30B (this page)1.6–4.3 µm
08 / Sources

Sources & disclaimer

Manufacturer datasheet values are starting points; optimal parameters depend on your substrate, equipment and environment. Product names and trademarks belong to their respective owners. NANYTE is not affiliated with the manufacturers listed. Last updated 2026-09-12.

Cite this recipe

NANYTE. "LOR 30B process recipe." NANYTE Photoresist Library. https://nanyte.com/photoresists/lor-30b. Accessed 2026-09-12.

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