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LOR 15B process recipe

LOR 15B coats 1.00-2.17 µm, filling the gap between LOR 10B and LOR 20B in the fast-dissolving B series.

https://nanyte.com/photoresists/lor-15b · last updated 2026-09-12

At a glance
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Manufacturer
MicroChem (MCC) — now Kayaku Advanced Materials
Tone
Not photoimageable (underlayer)
Chemistry
Ancillary (not photoimageable)
Thickness
1–2.2 µm
Exposure dose
Not exposed — dissolves in developer
Developer
No specific commercial developer product is named for this grade; the datasheet states LOR/PMGI is compatible with both metal-ion-free (TMAH) and metal-ion-bearing developer chemistries.
Applications
Lift-off

Cross-checked — two independent extractions agree on the spin curve and the single-value figures.

The underlayer is never exposed: it sits beneath an imaged top resist and the developer undercuts it laterally, leaving the overhang lift-off relies on. Schematic cross-sections for LOR 15B — feature width, film aspect ratio and sidewall angle are illustrative, not to scale.
01 / Coating

Spin coating

Spin curve for LOR 15B: film thickness in µm against spin speed in rpm.0.51.01.52.02.51k2k3k4kSPIN SPEED (rpm)THICKNESS (µm)
Data points
LOR 15B — film thickness (µm) by spin speed (rpm)
Seriesrpmµm
LOR 15B10002.2
15001.6
20001.4
25001.2
30001.1
35001.0
40001.0

Values are the manufacturer’s starting points, not a guarantee — characterize on your own tool. Series digitized from a published figure are approximate (±10 %).

read from figure — the red filled-square trace legended LOR 15B on the 'Thickness vs. Spin Speed - LOR B Thick Series' chart, p.5, the middle of the five traces. Seven plotted markers at 500 rpm intervals; no numeric table accompanies the chart.

Redrawn from the manufacturer's published data — hover to read between points, click to pin.
  • A well-behaved curve that lands on a round number at each end — 21,700 Å at 1000 rpm down to almost exactly 10,000 Å at 4000, so the grade covers a clean factor of two.
  • The knee sits around 1500-2000 rpm; below it thickness climbs quickly, above it the curve is nearly flat and speed buys little.
  • Coating parameters are published for the product line rather than per grade: 5 ml dispensed dynamically over 3-5 s onto a 150 mm wafer at 300-500 rpm, 10,000 rpm/s acceleration to a 3,000 rpm terminal speed, 45 s spin, with EBR PG for edge-bead and whisker removal.
Adhesion
HMDS not required — "Primers, such as HMDS, are typically not required" when LOR/PMGI is used as recommended; the datasheet describes excellent adhesion across semiconductor substrates. To dehydrate the surface first, bake at 200 °C for 5 min. LOR/PMGI is virtually insoluble in typical photoresist solvents, so a properly baked underlayer does not intermix with the imaging resist above it.
02 / Bake

Soft bake

Soft bake
Not published — characterize on-tool
Notes
The prebake dries the film and fixes its dissolution and undercut rate, and no grade-specific temperature or time is published. The recommended prebake range for the product line is 160-210 °C, hotplate preferred, and some PMGI products bake as high as 280 °C. Prebake temperature has the greatest influence on undercut rate, with prebake time, developer choice, develop mode and especially develop time behind it. On a B-series film that lever matters more than on an A grade because the starting dissolution rate is already high; conveniently, the published undercut-versus-bake curves (Figures 5a and 5b) are measured on LOR 10B, the nearest sibling to this grade in both series and thickness.
SOURCE: "Soft-Bake/Prebake Process" section and Figures 5a-5b, Kayaku…

"Soft-Bake/Prebake Process" section and Figures 5a-5b, Kayaku "LOR and PMGI Resists" technical data sheet, Rev. D (August 2023)

03 / Exposure

Exposure

LOR 15B is not photoimageable. It is not exposed at all — it is coated beneath an imaged top resist and undercut laterally during development. See the development step below.

04 / Development

Development

Developer
No specific commercial developer product is named for this grade; the datasheet states LOR/PMGI is compatible with both metal-ion-free (TMAH) and metal-ion-bearing developer chemistries.
Developer family
TMAH or buffered alkaline

Not published for this resist: Dilution, Time, Method, Rinse — characterize on-tool.

SOURCE: Product description, the LOR/PMGI process-flow section and the…

Product description, the LOR/PMGI process-flow section and the product selection guide, Kayaku "LOR and PMGI Resists" technical data sheet, Rev. D (August 2023)

05 / Post-processing

Hard bake, etch & strip

Stripper
Remover PG. EBR PG removes edge beads and whiskers and is also an effective spin-bowl cleaner and a rework solvent for unbaked wafers.
Storage
Store upright in original sealed containers in a dry area between 4 and 27 °C (40-80 °F), away from ignition sources, light, heat, oxidants, acids and reducers. Do not use after the expiration date.

Not published for this resist: Hard bake, Descum, Etch resistance — characterize on-tool.

06 / Applications

Where it's used

Practical notes from the datasheet

LOR 15B is a PMGI-based sacrificial underlayer from the fast-dissolving B series, spun beneath a conventional photoresist and never exposed. It sits between 10B and 20B, which makes it the grade for deposits in the one-to-two micron range that want B-series speed — a generous ledge opened quickly — without the extra thickness of 20B. The reason to want speed is mechanical: a thick deposit needs the underlayer to pull back far enough that the metal breaks cleanly at the edge rather than tearing. The reason to be careful with it is the same property seen from the other side, because a fast film keeps undercutting for as long as the imaging resist above is developing, and the datasheet singles out develop time as a particularly strong influence on where the ledge ends up. Of all the B grades, this one has the closest published characterisation to lean on: the undercut-versus-bake figures are measured on LOR 10B, its immediate neighbour.

07 / Family

Grades in this family

Other grades in the LOR B series line differ mainly in coating thickness:

LOR B series — grade comparison
GradeThickness
LOR 7B0.3–0.9 µm
LOR 10B0.7–1.6 µm
LOR 15B (this page)1–2.2 µm
LOR 20B1.3–3.5 µm
LOR 30B1.6–4.3 µm
08 / Sources

Sources & disclaimer

Manufacturer datasheet values are starting points; optimal parameters depend on your substrate, equipment and environment. Product names and trademarks belong to their respective owners. NANYTE is not affiliated with the manufacturers listed. Last updated 2026-09-12.

Cite this recipe

NANYTE. "LOR 15B process recipe." NANYTE Photoresist Library. https://nanyte.com/photoresists/lor-15b. Accessed 2026-09-12.

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