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LOR 10B process recipe

LOR 10B coats 0.65-1.57 µm and is the one LOR grade whose undercut behaviour the datasheet actually measures — both published undercut-versus-bake curves are taken on this film.

https://nanyte.com/photoresists/lor-10b · last updated 2026-09-12

At a glance
Download PDF
Manufacturer
MicroChem (MCC) — now Kayaku Advanced Materials
Tone
Not photoimageable (underlayer)
Chemistry
Ancillary (not photoimageable)
Thickness
0.7–1.6 µm
Exposure dose
Not exposed — dissolves in developer
Developer
No specific commercial developer product is named for this grade; the datasheet states LOR/PMGI is compatible with both metal-ion-free (TMAH) and metal-ion-bearing developer chemistries.
Applications
Lift-off

Cross-checked — two independent extractions agree on the spin curve and the single-value figures.

The underlayer is never exposed: it sits beneath an imaged top resist and the developer undercuts it laterally, leaving the overhang lift-off relies on. Schematic cross-sections for LOR 10B — feature width, film aspect ratio and sidewall angle are illustrative, not to scale.
01 / Coating

Spin coating

Spin curve for LOR 10B: film thickness in µm against spin speed in rpm.0.51.01.52.01k2k3k4kSPIN SPEED (rpm)THICKNESS (µm)
Data points
LOR 10B — film thickness (µm) by spin speed (rpm)
Seriesrpmµm
LOR 10B10001.6
15001.2
20001.0
25000.83
30000.72
35000.67
40000.65

Values are the manufacturer’s starting points, not a guarantee — characterize on your own tool. Series digitized from a published figure are approximate (±10 %).

read from figure — the light-blue filled-diamond trace legended LOR 10B on the 'Thickness vs. Spin Speed - LOR B Thick Series' chart, p.5. Seven plotted markers at 500 rpm intervals; no numeric table accompanies the chart.

Redrawn from the manufacturer's published data — hover to read between points, click to pin.
  • The curve runs 15,700 Å at 1000 rpm down to 6,500 Å at 4000 rpm and is nearly flat above 3000 rpm, so speed stops being a useful control below about 0.7 µm — the grade below is the better answer there.
  • A convenient landmark: 1.00 µm falls at 2000 rpm, near the middle of the usable range.
  • Coating parameters are published for the product line rather than per grade: 5 ml dispensed dynamically over 3-5 s onto a 150 mm wafer at 300-500 rpm, 10,000 rpm/s acceleration to a 3,000 rpm terminal speed, 45 s spin, with EBR PG for edge-bead and whisker removal.
Adhesion
HMDS not required — "Primers, such as HMDS, are typically not required" when LOR/PMGI is used as recommended; the datasheet describes excellent adhesion across semiconductor substrates. To dehydrate the surface first, bake at 200 °C for 5 min. LOR/PMGI is virtually insoluble in typical photoresist solvents, so a properly baked underlayer does not intermix with the imaging resist above it.
02 / Bake

Soft bake

Soft bake
Not published — characterize on-tool
Notes
This is the grade the datasheet actually characterises: Figure 5a plots undercut rate against soft-bake temperature and Figure 5b plots it against soft-bake time, both measured on LOR 10B. The recommended prebake range for the product line is 160-210 °C, hotplate preferred, and some PMGI products bake as high as 280 °C. The text singles out prebake temperature as the greatest influence on undercut rate, ahead of prebake time, developer choice, develop mode and — particularly — develop time. Neither figure is reduced to a table, so the curves give direction and shape rather than a number to dial in: hotter and longer both slow the dissolution and tighten the undercut. No single recommended prebake temperature or time is published for this or any other grade.
SOURCE: "Soft-Bake/Prebake Process" section and Figures 5a-5b, Kayaku…

"Soft-Bake/Prebake Process" section and Figures 5a-5b, Kayaku "LOR and PMGI Resists" technical data sheet, Rev. D (August 2023)

03 / Exposure

Exposure

LOR 10B is not photoimageable. It is not exposed at all — it is coated beneath an imaged top resist and undercut laterally during development. See the development step below.

04 / Development

Development

Developer
No specific commercial developer product is named for this grade; the datasheet states LOR/PMGI is compatible with both metal-ion-free (TMAH) and metal-ion-bearing developer chemistries.
Developer family
TMAH or buffered alkaline

Not published for this resist: Dilution, Time, Method, Rinse — characterize on-tool.

SOURCE: Product description, the LOR/PMGI process-flow section and the…

Product description, the LOR/PMGI process-flow section and the product selection guide, Kayaku "LOR and PMGI Resists" technical data sheet, Rev. D (August 2023)

05 / Post-processing

Hard bake, etch & strip

Stripper
Remover PG. EBR PG removes edge beads and whiskers and is also an effective spin-bowl cleaner and a rework solvent for unbaked wafers.
Storage
Store upright in original sealed containers in a dry area between 4 and 27 °C (40-80 °F), away from ignition sources, light, heat, oxidants, acids and reducers. Do not use after the expiration date.

Not published for this resist: Hard bake, Descum, Etch resistance — characterize on-tool.

06 / Applications

Where it's used

Practical notes from the datasheet

LOR 10B is a PMGI-based sacrificial underlayer from the fast-dissolving B series, and it is the grade worth knowing about even if you end up buying a different one: every published undercut measurement on this datasheet was made on LOR 10B. Figures 5a and 5b show undercut rate against prebake temperature and against prebake time, and the text singles out temperature as the strongest influence. No other grade gets that treatment, so anyone tuning an A or C grade is reading a B-grade curve and scaling by judgement. On thickness it sits in the middle of the B line at 0.65-1.57 µm. The B series dissolves faster than A for the same prebake, which is right when the deposited metal is thick and needs a generous ledge to break at, and wrong when the feature is fine — the undercut keeps running for as long as the imaging resist above is developing, and develop time is the variable the datasheet flags as especially influential.

07 / Family

Grades in this family

Other grades in the LOR B series line differ mainly in coating thickness:

LOR B series — grade comparison
GradeThickness
LOR 7B0.3–0.9 µm
LOR 10B (this page)0.7–1.6 µm
LOR 15B1–2.2 µm
LOR 20B1.3–3.5 µm
LOR 30B1.6–4.3 µm
08 / Sources

Sources & disclaimer

Manufacturer datasheet values are starting points; optimal parameters depend on your substrate, equipment and environment. Product names and trademarks belong to their respective owners. NANYTE is not affiliated with the manufacturers listed. Last updated 2026-09-12.

Cite this recipe

NANYTE. "LOR 10B process recipe." NANYTE Photoresist Library. https://nanyte.com/photoresists/lor-10b. Accessed 2026-09-12.

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