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NR9-1000PY process recipe

NR9-1000PY is Futurrex's thinnest NR9 lift-off resist, coating about 0.75–2.0 µm between 800 and 5000 rpm and giving a negative-sloping sidewall at 365 nm. Its sensitivity is quoted at 390 mJ/cm² for a 1 µm film, and the 1 µm develop is about 10 s in RD6.

https://nanyte.com/photoresists/nr9-1000py · last updated 2026-10-15

At a glance
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Manufacturer
Futurrex, Inc.
Tone
negative
Thickness
0.8–2 µm
Exposure dose
390 mJ/cm² at 365 nm (per 1 µm film)
Developer
Resist Developer RD6
Applications
Lift-off

Cross-checked — the spin curve (where published) and the single-value figures were read twice, independently, from the datasheet, with any disagreement settled against it.

The exposed resist stays after development with an undercut sidewall — the overhang a lift-off needs; the unexposed film dissolves. Schematic cross-sections for NR9-1000PY — feature width, film aspect ratio and sidewall angle are illustrative, not to scale.
—01 / Coating

Spin coating

Spin curve for NR9-1000PY: film thickness in µm against spin speed in rpm.0.51.01.52.02.51k2k3k4k5kSPIN SPEED (rpm)THICKNESS (µm)
Data points
NR9-1000PY — film thickness (µm) by spin speed (rpm)
Seriesrpmµm
NR9-1000PY8002.0
20001.2
30001.0
40000.86
50000.75

Values are the manufacturer’s starting points, not a guarantee — characterize on your own tool.

numeric table 'Film thickness after 150°C hotplate bake for 60 s. / Coating spin speed, 40 s spin (rpm): (nm)', p.1 of Futurrex NR9-1000PY Technical Information. The datasheet prints each point as an nm range; each point here is the exact midpoint of that range, converted nm to µm. Printed ranges: 800 rpm = 1900-2100 nm, 2000 rpm = 1170-1290 nm, 3000 rpm = 950-1050 nm, 4000 rpm = 817-903 nm, 5000 rpm = 712-788 nm. The 3000 rpm midpoint (1000 nm) matches the '1000' in the product name.

Redrawn from the manufacturer's published data — hover to read between points, click to pin.
  • Spin for 40 s at the chosen speed; the table assumes a 150 °C, 60 s hotplate bake afterwards.
  • Edge Bead Remover EBR2 is dispensed on both faces of the spinning substrate through nozzles 0.5–1.0 cm from the edge, starting as soon as the bead forms (3–5 s after the resist dispense stops) and ending 5 s before the spin cycle finishes.
  • Bake times in the sheet are for substrates that conduct heat well (Si, GaAs); multiply them by 3.5 for poor conductors such as glass.
Adhesion
Not addressed in this datasheet.
—02 / Bake

Soft bake

Soft bake
150 °C · 60 s · hotplate
Notes
For good thermal conductors (Si, GaAs); multiply bake times by 3.5 on poor conductors such as glass. No alternate schedule is printed for this grade.

SOURCE: Processing step 3, p.2; also the Properties heading, p.1 of Futurrex NR9-1000PY Technical Information

—03 / Exposure

Exposure dose

The manufacturer publishes 390 mJ/cm² at 365 nm (per 1 µm film). Dose scales with film thickness and depends on your optics, so treat it as a starting point and run a dose array.

Dose at 365 nm
390 mJ/cm² (per 1 µm film)
Dose at 405 nm
Not published — characterize on-tool
As published
390 mJ/cm² at 365 nm is the only exposure figure Futurrex prints for this resist, quoted for a 1 µm film. There is no h-line number and no scaling rule for other thicknesses.
Post-exposure bake
100 °C · 60 s
SOURCE: NR9-1000PY Technical Information

Properties, p.1 of Futurrex NR9-1000PY Technical Information: 'Sensitivity at 365 nm exposure wavelength (mJ/cm² for 1 µm thick film) 390'

—04 / Development

Development

Developer
Resist Developer RD6
Dilution
RD6/water 3:1 to slow development (55 s for a 1 µm film)
Time
10 s
Method
spray or immersion
Rinse
Deionized water rinse until water resistivity reaches the prescribed limit (Processing step 7).
Developer family
TMAH-based

SOURCE: Processing steps 6-7, p.2 of Futurrex NR9-1000PY Technical Information

—05 / Post-processing

Hard bake, etch & strip

Stripper
Resist Remover RR4 at 110 °C, or acetone (Processing step 9, p.2).
Storage
"Guaranteed shelf life at 25°C storage (years) 3" (Properties, p.1); "shelf life exceeding 3 years at room temperature storage" (Description, p.1).

Not published for this resist: Hard bake, Descum, Etch resistance — characterize on-tool.

—06 / Applications

Where it's used

Practical notes from the datasheet

NR9-1000PY is the thin end of Futurrex's NR9 negative line: a cyclohexanone-based resist, 19–23 % solids, exposed at 365 nm and developed in basic aqueous RD6. The sheet says the developed profile has a negative slope that suits lift-off, and that the amount of undercut can be adjusted through exposure energy. Product code and table agree: '1000' is the 3000 rpm point (950–1050 nm). Dose is 390 mJ/cm² for a 1 µm film, roughly twice the figure Futurrex prints for NR9-1500PY, so do not carry a dose across grades. The softbake is 150 °C for 60 s and the PEB is 100 °C for 60 s, both for silicon-like substrates; on glass the datasheet multiplies bake times by 3.5. Temperature resistance is quoted up to 100 °C, which matters if later steps run hot.

—07 / Troubleshooting

Troubleshooting

Common failure modes for NR9-1000PY, answered from the manufacturer's datasheet and application notes. These are starting points — your substrate, tooling and environment shift the specifics, so calibrate on-tool.

How do I adjust the lift-off undercut with NR9-1000PY?

The sheet lists easy adjustment of the undercut through exposure energy as an advantage of this resist. The developed sidewall slopes negatively, which is what makes lift-off simple. The flow is 150 °C/60 s softbake, 365 nm exposure, 100 °C/60 s PEB, RD6 develop, then strip in RR4 at 110 °C or acetone.

SOURCE: Futurrex NR9-1000PY Technical Information — Description, p.1, and Processing steps 3-9, p.2

How do I slow the NR9-1000PY develop down?

Neat RD6 clears a 1 µm film in about 10 s by spray or immersion. Mixing RD6 with water 3:1 stretches that to about 55 s for the same film, which gives a more controllable develop. Rinse in deionized water until the resistivity reaches your limit.

SOURCE: Futurrex NR9-1000PY Technical Information — Processing steps 6-7, p.2

Do the bake times change on glass substrates for NR9-1000PY?

Yes. The 150 °C softbake and 100 °C PEB are written for good thermal conductors such as silicon and GaAs. For poor conductors such as glass the sheet says to increase bake times by a factor of 3.5.

SOURCE: Futurrex NR9-1000PY Technical Information — Processing note, p.2

—08 / Sources

Sources & disclaimer

Manufacturer datasheet values are starting points; optimal parameters depend on your substrate, equipment and environment. Product names and trademarks belong to their respective owners. NANYTE is not affiliated with the manufacturers listed. Last updated 2026-10-15.

Cite this recipe

NANYTE. "NR9-1000PY process recipe." NANYTE Photoresist Library. https://nanyte.com/photoresists/nr9-1000py. Accessed 2026-10-15.

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Expose it at 365 and 405 nm

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BEAM exposes at 365 nm, the wavelength this resist's datasheet specifies a dose for — writing lift-off masks in it directly, no photomask, down to <0.4 µm features.

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