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AZ nLOF 2070 process recipe

AZ nLOF 2070 is the ~7 µm grade of AZ's chemically amplified negative-tone nLOF 2000 series, engineered for single-layer lift-off with a required post-exposure bake, no rehydration wait, and thermal stability above 150°C for its lift-off undercut sidewall.

https://nanyte.com/photoresists/az-nlof-2070 · last updated 2026-07-10

At a glance
Manufacturer
Merck
Tone
negative
Chemistry
Chemically amplified
Thickness
5.3–11.8 µm
Developer
AZ 300MIF
Applications
Lift-off · Etch mask
Etch maskSuitable forLift-offSuitable for

Cross-checked — two independent extractions agree.

01 / Coating

Spin coating

AZ nLOF 2070 is spin-coated to 5.3–11.8 µm. The curve below is redrawn from the manufacturer's published data — read your target thickness off the vertical axis and take the matching spin speed as a starting point.

Spin curve for AZ nLOF 2070: film thickness in µm against spin speed in rpm.0.005.01015201k2k3k4kSPIN SPEED (rpm)THICKNESS (µm)
Data points
AZ nLOF 2070 — film thickness (µm) by spin speed (rpm)
Seriesrpmµm
AZ nLOF 207050012
100011
15009.2
20007.8
25007.0
30006.3
35005.8
40005.3

Values are the manufacturer's starting points, not a guarantee; verify on your own tool. Characterize on-tool. Series digitized from a published figure were independently cross-checked by a second blind read; treat those values as approximate (±10 %).

read from figure, "SPIN CURVES (150mm Silicon)", p.1 of AZ nLOF 2000 Series Technical datasheet (Rev. 03/21) — chart plots three grades (nLOF 2070 red, nLOF 2035 yellow, nLOF 2020 blue) with an explicit color-coded legend; nLOF 2070 identified by its red 'nLOF 2070' legend entry (top curve, highest thickness at every speed) and cross-checked against the grade-specific 7.0 µm reference process (p.5, which names 'AZ nLOF 2070 (330cPs)' explicitly).

Redrawn from the manufacturer's published data — hover to read values between points, click to pin.

Unlike the ambiguous combined charts flagged elsewhere in this recipe set, this chart carries an explicit color-coded legend naming each of the three plotted grades individually (nLOF 2070, nLOF 2035, nLOF 2020), and the identification is cross-checked against this datasheet's own grade-specific reference-process tables (p.3, p.5), which name the exact grade and viscosity (cPs) used for each nominal film thickness. Still a figure read, not a numeric table, so visual QC is required. No dispense volume, spin ramp, or edge-bead detail is published in this datasheet.

Adhesion
HMDS recommended — Oxide-forming substrates (e.g. Si) should be HMDS primed prior to coating (PROCESS CONSIDERATIONS > SUBSTRATE PREPARATION, p.8). The 7.0 µm reference process specifies a vapor prime of HMDS 140°C/60s (p.5).
Rehydration
None required — p.1 TYPICAL PROCESS states 'Rehydration Hold: None', consistent with this being a chemically amplified resist, not a DNQ resist. The 7.0 µm reference process (p.5) likewise lists 'Post Bake Delay: None'. (Source: TYPICAL PROCESS, p.1, and EXAMPLE PROCESS (7.0µm Film Thickness on Si), p.5, of AZ nLOF 2000 Series Technical datasheet (Rev. 03/21))
02 / Bake

Soft bake

Soft bake
110 °C · 1.5 min · hotplate
Notes
Reference process for the 7.0 µm nLOF 2070 film (p.5): 110°C, 90 s, direct contact hotplate — longer than the 60 s used for the thinner 2.0 µm (nLOF 2020) and 3.5 µm (nLOF 2035) grades, consistent with a thicker coat needing more bake time to drive off solvent. Series-level guidance (p.8) puts soft bake temperature generally in the 100-110°C range.

SOURCE: EXAMPLE PROCESS (7.0µm Film Thickness on Si), p.5 of AZ nLOF 2000 Series Technical datasheet (Rev. 03/21)

03 / Exposure

Exposure dose

The manufacturer does not publish a clearing dose for AZ nLOF 2070. Determine it with a dose array on your own tool.

As published
"Expose: i-line @ various doses (0.54NA) Nikon Stepper" — verbatim, EXAMPLE PROCESS (7.0µm Film Thickness on Si), p.5. Confirmed series-wide: "AZ nLOF 2000 requires exposure energy at the 365nm wavelength" (p.8).
Post-exposure bake
110 °C · 1.5 min

Not published for this resist: Dose at 365 nm, Dose at 405 nm — characterize on-tool.

04 / Development

Development

Developer
AZ 300MIF
Dilution
undiluted (ready-to-use 0.26N / 2.38% TMAH developer; no dilution ratio stated)
Time
2 min
Method
puddle
Rinse
Not published — characterize on-tool
Developer family
TMAH-based

SOURCE: EXAMPLE PROCESS (7.0µm Film Thickness on Si), p.5 of AZ nLOF 2000 Series Technical datasheet (Rev. 03/21): 'AZ 300MIF, 2 x 60 second puddles'

05 / Post-processing

Hard bake, etch & strip

Stripper
AZ 400T or AZ Remover 770 (solvent-based removers), recommended per PROCESS CONSIDERATIONS > STRIPPING, p.8 of AZ nLOF 2000 Series Technical datasheet.

Not published for this resist: Hard bake, Descum, Etch resistance, Storage — characterize on-tool.

SOURCE: PROCESS CONSIDERATIONS > HARD BAKE, and HARD BAKE STABILITY for Large Pads in AZ nLOF™ 2070 (7.0µm Film Thickness), p.8 of AZ nLOF 2000 Series Technical datasheet (Rev. 03/21)

06 / Applications

Where it's used

Lift-offEtch mask

AZ nLOF 2070 is the ~7 µm grade of AZ's nLOF 2000 series, a chemically amplified negative photoresist purpose-built to replace older image-reversal and multi-layer lift-off processes with a single expose/PEB/develop flow and a clean undercut sidewall. As with the whole series, the post-exposure bake is required, not optional, unlike the DNQ positive resists elsewhere in this recipe set, and CD is sensitive to PEB temperature (roughly <0.04 µm/°C per the datasheet's series-level guidance). Unlike thick DNQ positive resists it needs no rehydration wait after softbake, and softbake/PEB both scale up to 90 s at this thickness versus 60 s for the thinner 2020/2035 grades. It develops in AZ 300MIF (0.26N/2.38% TMAH) via two 60-second puddle cycles rather than one. Printed features are thermally stable well above 150°C — the datasheet specifically demonstrates hard-baking large 7 µm nLOF 2070 pads at 115-130°C with stable edge profiles — which is what lets nLOF's negative-tone undercut survive a subsequent metal evaporation and lift-off step. The datasheet explicitly does not recommend nLOF 2000 series resists for use on copper substrates.

07 / Sources

Sources & disclaimer

Research using this resist
  1. Gerlt et al.. Reduced Etch Lag and High Aspect Ratios by Deep Reactive Ion Etching (DRIE). Micromachines (2021). doi:10.3390/mi12050542
    7.2 µm nLOF 2070 DRIE mask; documents its slightly angled sidewalls
  2. Huang et al.. Fabrication of metal air bridges for superconducting circuits using two-photon lithography. Applied Physics Letters (2025). doi:10.1063/5.0271788
    7 µm nLOF 2070 air-bridge lift-off for superconducting qubit circuits, direct-write patterned

Manufacturer datasheet values are starting points; optimal parameters depend on your substrate, equipment and environment. Product names and trademarks belong to their respective owners. NANYTE is not affiliated with the manufacturers listed. Last updated 2026-07-10.

Cite this recipe

NANYTE. "AZ nLOF 2070 process recipe." NANYTE Photoresist Library. https://nanyte.com/photoresists/az-nlof-2070. Accessed 2026-07-10.

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